Dr E. Ramanathan PhD | WhatsApp Training Contact: 9444929163
SaitechAI — Solids (Non-Volatile) % Calculator Binder / Resin / Paint
Compute solids by mass from oven-loss data and follow standard test procedures with ASTM/ISO/BIS references.
Interactive Calculator
Use either the pan method (preferred) or direct sample/residue masses.
Report temperature & time with every result
Typical: 110 ± 5 °C for 60 min (ASTM D2369). For varnishes, see ASTM D1644 schedules.
Record any deviations (thick films, reactive systems, etc.).
Sample taken—
msample
Residue (non-volatile)—
mresidue
Solids by mass—
% non-volatile
Test Procedure (Oven Loss)
- Prepare representative sample (mix gently; avoid air entrapment). Follow BIS sampling guidance.
- Dry, clean, and precondition weighing pan or aluminium dish; record mass Wp (±0.001 g).
- Weigh ~1–2 g of material (high-solids may use ≤1 g). Record W1 (pan + wet).
- Spread as a thin uniform film to accelerate solvent release.
- Oven: 110 ± 5 °C for 60 min (typical for coatings per ASTM D2369). Varnishes: see ASTM D1644 schedules.
- Cool in desiccator (10–15 min) and weigh W2 (pan + dry).
- Calculate Solids % =
((W₂−Wₚ)/(W₁−Wₚ))×100. Volatile % = 100 − Solids %. - Run duplicate determinations; report mean and conditions (temp/time, atmosphere, any inhibitors).
Notes & good practice
- Highly reactive systems (2K PU/epoxy) may cure further; use shortest feasible time; record gel/skin formation.
- Water-borne with coalescents: ensure full removal; if foaming, extend time or use step temperature with caution.
- If splatter/volatilization occurs, use covered dish with vent or reduce sample mass.
- Report density separately if you need volume solids (ISO 3233 route).
Standards & References
- ASTM D2369 — Volatile content of coatings (110 ± 5 °C, 60 min typical). Inverse gives % non-volatile (solids). :contentReference[oaicite:0]{index=0}
- ASTM D1644 — Non-volatile content of varnishes (procedures & schedules). :contentReference[oaicite:1]{index=1}
- ISO 3251:2019 — Determination of non-volatile-matter content by mass for paints/varnishes/binders. :contentReference[oaicite:2]{index=2}
- BIS IS 101 (Part 2/Sec 2) — Chemical examination: Volatile matter (use inverse for solids %). :contentReference[oaicite:3]{index=3}
- BIS IS 101 (Part 8/Sec 2) — Pigments & non-volatile matter in paints/related products. :contentReference[oaicite:4]{index=4}
- For volume-solids & spreading rate: ISO 3233-1. :contentReference[oaicite:5]{index=5}
Always cite the exact edition/date used in your COA/QC report.
© SaitechAI • Result validity depends on correct sampling, oven conditions, and duplicate agreement (≤0.5 % absolute recommended for routine QC).
